The Distillation of Thymus Vulgaris Essence to Demonstrate TBP Curve

Abstract

Based on a research project on Shirazi Thymus of the Eksir Gol Sorkh company, the essence of this Thymus included five main components, which based on the results gained from GC device, there are 5 main components in this Thymus namely ?-Pinene, ?-Terpinene, P-Cymen, ?-Terpinen, and Thymol, each of which has a percentage as follows 1.118, 3.831, 25.815, 14.771, and 54.465. With increasing the amount of Distillation, more Thymol can be achieved, and in this experiment, the amount of Thymol increases 18 percent to 92 percent. With passing of 81min from the 170 degrees Celsius, the temperature of essence solution, which is a stable 250 degrees Celsius in Heating (Oil/sand) bath, reaches 240 degrees Celsius. With an increase in the volume of Distillation material, the output water of condenser reaches up to 22.7 degrees Celsius from 21.9 degrees Celsius in such a way that incoming cold-water temperature has increased up to 21.9 degrees Celsius from 21.4 degrees Celsius by passing of time. In TBP diagram, with an increase in Distillation volume from 2 percent to 72 percent, the boiling temperature of Thymus essence solution has reached 240 degrees Celsius from 160 degrees Celsius.

KEYWORDS: Distillation; Thymus; TBP; GC